Nickel Insitute - Nickel Alloys in Organic Acids & Related Compounds

TABLE XLV

TABLE XLVII

Corrosion of Stainless Steel in a Propionic Acid-Anhydride Mixture

Corrosion of Proprietary Alloys in 2-Ethyl Butyric Acid

Duplicate specimens exposed for 48 hours or longer in refined boiling acid without aeration or deaeration.

Conditions: Specimens exposed in pressure equipment at 260 ºC (500 ºF) and 300 atmospheres pressure from 4 to 7-hour periods in a 65% propionic acid/35%propionic anhydride mixture with continuous feed of two liters/ hour.

Corrosion Rate

Alloy

mm/y

mpy

Corrosion Rate

.03 .05 <.03 .89 .18 .28 .03 <.03 .03 5.33 <.03

1 2

Type 316 Stainless Steel CRUCIBLE alloy 223 Titanium WAUKESHA 23 WAUKESHA 54 WAUKESHA 88 KROMARC 55 E-BRITE 26-1 CRUCIBLE 26-1 CROLOY 16-1 CARPENTER alloy 20Cb-3

Alloy

Liquid

Vapor

mm/y mpy mm/y

mpy

<1 35 7 11 1 <1 1 210 <1

129.41 141.86

5095 5585

80,01 78.10 116.84

3150 3075 4600

Type 430 Stainless Steel Type 304 Stainless Steel Type 347 Stainless Steel Type 316 Stainless Steel Type 316 Stainless Steel (Sen.)

3.63 9.91 12.01

143 390 475 179 313 286

7,09 4.01 2.44 7.65 8.36

279 158 96 301 329

Type 317 Stainless Steel Type 318 Stainless Steel CARPENTER alloy 20

4.55 7.95 7.26

TABLE XLVI

Corrosion of Alloys in Higher Organic Acids

Conditions: Laboratory tests for 48 hours at temperatures shown in refined (99.9+) acids.

Corrosion Rate

Acid (Approximate

Test

Silicon Bronze

Type 304 Stainless Steel

Type 316 Stainless Steel

Carbon Steel

Copper

boiling point)

Temperature

ºC

ºF mm/y mpy mm/y mpy mm/y mpy mm/y mpy mm/y mpy

Acetic (116 ºC or 240 ºF)

26 78.8

2.79 5.33

110 210

.28 .08 .05

11

.41 .08 .15

16

<.03

<1 10 <1 <1 45 <1 <1 <1 21 5

<.03

<1

116

240

3 3

3 6

.25

.08

3

.71

28 78

<.03

<.03 <.03 <.03 <.03 <.03 <.03 <.03 .10

<1 <1 <1 <1 <1 <1 <1 4

Propionic (140 ºC or 284 ºF)

26 78.8

110

240

1.98

2.13

84 Nil

3.40

134

.13

.15

6 – 2

Nil

.05

2 – 2 5 1 9

<.03 1.14 <.03 <.03 <.03

Butyric (163 ºC or 325 ºF)

26 78.8

163

325

– 2

.05

.05

.05 .13 .03 .23

Valeric (185 ºC or 365 ºF)

26 78.8

140

284

1.37

54

2.06

27

.18 .86

7

.03 .41

1

2-Ethylbutyric (190 ºC or 374 ºF)

26 78.8

150

302

34

16

.53

2-Methylpentanoic (195 ºC or 383 ºF)

.03 .53

1

.08 .30

3

.10 .08

4 3

<.03 <.03

<1 <1

<.03 <.03

<1 <1

26 78.8

150

302

21

12

2-Ethylhexanoic

.03

1

<.03 <.03

<1 <1

<.03 <.03

<1 <1

<.03

<1

<.03 <.03 <.03 <.03 <.03 <.03

<1 <1 <1 <1 <1 <1

(220 ºC or 428 ºF)

26 78.8

190

374

1.27

50

.20

8

.03 .89 .03 .84

1

05

2

.03

1

<.03

<1 17 <1

Iso-octanoic (240 ºC or 464 ºF)

26 78.8

190

374

35 <1 33

<.03 <.03 <.03

<1 <1 <1

<.03 <.03 <.03

<1 <1 <1

.43

<.03

Iso-decanoic (265 ºC or 509 ºF)

26 78.8

.20

8

190

374

Reference 5

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